부산대학교 공동실험실습관
미래를 향한 힘찬 발걸음
부산대학교 공동실험실습관
미래를 향한 힘찬 발걸음
공유
인쇄
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| 모델명 | SMART BREEZE |
| 설치장소 | 구조분석실 (303) |
| 설치상태 | 고정 |
| 장비상태 | 불용처리 |
| 문의처 | TEL : 051-510-3404 E-mail : mjjeen@gmail.com |
| 오퍼레이터 | 불용장비 |
예약정보
예약가능요일 : 월요일, 화요일, 수요일, 목요일, 금요일,
예약최소/최대시간/(예약단위당)예약가능건수 : 1일 / 30일 / 100건
예약가능기간 : 현재일로부터 1개월까지
제약사항 : 당일예약불가, 당일취소불가
| 1. Charge-Coupled Device area detector for Single Crystal x-x-x-x-x-x-x-x-frame data collection and imaging. 2. The Ultimate Solutions for Chemical Crystallography, 4K CCD detector and 1:1 demagnification ration has no image distortion. 3. Automates sample loading and unloading the sample for data acquisition. 4. 3D-algorithm data integration which processes data x-x-x-x-x-x-x-x-frames and generates datasets of intensities for structure solution and refinement. Support for twinned and modulated structures. 5. High sensitivity, no spatial distortion, lower noise, higher throughput, higher dynamic range scientific grade CCD chip |
| 1. CCD Area Detector 1) Charge-Coupled Device area detector 2) Number of pixels : 4096 x 4096 3) Active Area : 62mm x 62mm 4) CCD Pixel size : 15 𝝻 m x 15𝝻 m 5) Demagnification Ratio : 1:1, no distortion 6) Typical Quantum Gain : 170 electrons/X-Ray photon 7) Readout port : 2 port 8) Air-cooled 4K CCD detector
2. X-RAY SOURCE 1) 50 W Microfocus tube * 50KV, 1mA 2) Doubly curved crystal * For Point focus 3) High voltage generator * Power : 50kV 1mA * Controller for failsafe safety/experiment shutter 3. Goniometer and Sample loader Detector distance and 2-Theta offset angle optimized for acquisition of crystallographic data from molybdenum radiation to IUCR standards 1) Omega: * Range : 180 deg 2) Phi * Range :360 deg * 0.5 deg step size * Reproducibility 0.001 deg 3) Chi * Range : Fixed angle 4) Automated sample loader * Automates sample loading and unloading the sample for data acquisition * Reproducibility 30 Micrometer 5) Goniometer head * Automatically sample centering in head 6) Safety * Interlocked radiation enclosure: * Compact radiation enclosure inside the instrument cover * Instrument enclosure includes an "X-RAY ON" indicator and shutter interlocks. 4. Single Crystal XRD Software 1) Control Software: * Fully automated software with a "Kiosk style" graphical user interface (GUI). Interaction through a touch-screen interface. * GUI does not require any crystallographic knowledge, only an approximate sum formula is required to facilitate structure determination. Optional information can be provided for report generation. The GUI provides constant feedback about the status and the quality of the structure determination. * The GUI interacts with "automation platform" which performs all necessary steps for a structure determination. These include determination of: crystal quality, unit cell, Bravais type data acquisition exposure time, data collection strategy, data integration and continued quality monitoring, scaling and absorption correction, spacegroup determination, structure solution and refinement. Underlying software packages are the SHELXTL suite of programs cell_now (indexing), SADABS (Scaling and absorption correction), XPREP (space group determination), XM, XS (structure solution), XL(structure refinement), SAINT (data integration) and GIS (Instrument control) * Fully automated html report generation * Fully automated archiving using CD-ROM. CD-ROM contains all raw and preliminary data for further processing using software. |
| 단결정 X-선 3차원 분자 구조해석 |
| 1. 기기 담당자와 시료의 측정 및 분석 가능여부 점검 (우선연락 필수!)
2. 신청서 작성 후 접수 3. 시료 측정 (전처리-측정-구조해석) 4. 이용료 납부 후 결과 통보 5. 기자재 이상유무 확인 |
| 기초분석: 20,000원/시료
전처리: 50,000원/시료 실온측정: 100,000원/시료 저온측정: 150,000원/시료 구조분석: 300,000원/시료(40개 원자 기준임. 원자 추가시 5,000원/원자) |
| H. Lee, T. H. Noh, O.-S. Jung, Angew. Chem. Int. Ed. 2016, 55, 1005.
T. H. Noh, H. Lee, J. Jang, O.-S. Jung, Angew. Chem. Int. Ed. 2015, 54, 9284. H. Lee, T. H. Noh, O.-S. Jung, Angew. Chem. Int. Ed. 2013, 52, 11790. |